Lithium tri-t-butoxyaluminium hydride
CAS NO.:17476-04-9
Molecular formula:LiAl(OC4H9)3H
Molecular weight:254.27
Quality index
Specification | Appearance | Quality Index |
Specification 1 | White powder | Assay: 98%min. |
Specification 2 | Colorless or light grey liquid | Concentration: 1±0.02M in THF |
Properties
This product sublimes at 280℃ under vacuum. It is soluble in dimethoxyethane, diglyme and THF, and slightly soluble in diethyl ether. It is stable in dry air but it can be hydrolyzed in moist air. This product is a mild high selective reducing agent, which can reduce ketones, aldehydes and acyl chloride in diethyl ether or diethylene glycol at 0℃. It can’t reduce aliphatic acid ester and nitrile, but can reduce phenyl esters of aliphatic acid and alicyclic acid.
Usage
It is used as reducing agent in organic synthesis of pharmaceuticals, perfumes, pesticides, dyes and other fine chemicals. It was widely used in reducing steroid ketone. It is used as the reducing agent for synthesizing Azanavir, which is an anti-AIDS API.
Packing
1) 100g/Tin; 500g/ Tin; 20kg/Barrel
2) 100ml/Glass bottle; 500ml/Glass bottle; 1L/Glass bottle; 60L/Stainless steel barrel; 70L/Stainless steel barrel; 100L/Stainless steel barrel
Storage
Avoid breakage and moisture, far away from heat, fire and inflammable matter, no mix with acid, oxidant and substance containing water. Stored in a sealed container, and kept in cool, dry, well-ventilating chemical warehouse.
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